I have peppermint/mint growing in my garden backyard. I want to make Ice Cream for children and they are asking for some flavour paan ice cream in Hindi (mint ice cream) and for that I want Menthol powder to mix into plain ice cream. How can I make Menthol Powder from Mint/Peppermint Leaves?
How to extract menthol powder from fresh mint/peppermint
chemistryextractsmint
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Best Answer
This is a fun question, but your plan is not very practical.
If you indeed insist on doing it, you have three steps in the process of menthol extraction:
For the essential oil extraction, the only method doable at home is a steam/water distillation. (OK, there are also absolue methods, but they are less practical, and not necessary for mint). So you are left with a mixture of a hydrosol and mint essential oil.
Here is where it becomes difficult: the second step is to separate the oil from the hydrosol. Most methods I know of will produce something which is not food-safe. The popular ones are to use a nonpolar solvent and then boil it off (I hope you don't plan on handling diethyl ether in your kitchen!) but I also found a reference to "passing it through a bed of anhydrous sodium sulphate". This is probably your best bet edibilitywise, but getting the supplies and learning the process won't be easy.
In the end, you have to freeze the essential oil to a sufficiently low temperature (the source with the sodium sulphate uses -60 C but I also found references to -22), then keep it for a few days and harvest the crystals.
If you are brave enough to do it at home (and live in a place where it is not illegal to have a distillation still, and found a freezer that goes to -22) you will need time, space for the apparatus, and mint. Lots of mint. Here I found an article for a portable still which weighs 635 kg, has a 500 l distillation tank, can process up to 9 kg dried mint per distillation (you'll first need an area where you can hang 72 kg of fresh mint to dry out for a month or two, or find a dehydrator and pay for the energy to process it) and yields about 100 ml of essential oil from peppermint, half that if you use spearmint. The oil consists of about 50% menthol, but I couldn't find references for the actually recovered amount when using crystalization only (chemists tend to follow up with a boric acid distillation) but let's say you can recover half of the contained menthol, this would be 15-25 grams of pure menthol crystals.
If your children want just a few portions of ice cream, you should be able to downscale this to 1/10 or less, and get away with a much smaller still. But you'll still need several square meters worth of mint plants, and your children will have to wait a few weeks for their ice cream.